Instruction Manuals

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Varian NMR Instruments:

• Routine Operation of the Varian NMRs using VNMRj 3.2A 
• 1D NMR Experiments.
• 2D NMR Experiments. 
• Variable Temperature Operation
• New VNMRj Software : Processing/Plotting (from Agilent Manual)
• DOSY: Diffusion Ordered NMR Spectroscopy (Wide variety of methods available)
  • Ask for consultation and instruction in these methods
• Decoupling Protons when observing Heteronuclei (Varian instruments Only)
  • Gating Decoupler On or Off (Varian instruments only)

​Bruker Avance-III 400 NMR in JSCBB C1B82:

• Using ICON-NMR in Automation for the JSCB 400

Bruker Avance-III 300 NMR:

• Using ICON-NMR in Automation on the 300

General Information about NMR & Utilities:

• Locking and Shimming (general concepts, manual locking & shimming)
• Relaxation and Quantitation (Integration)... how long do you have to wait between scans?
• Dynamic NMR Experiments - Practice and Calculations : Chemical/Conformational Exchange
  • 2D & 1D-selective EXCHSY (exchange spectroscopy)
• Sample Temperature Calibration for VT NMR
• NMR Probe Tuning: What Every NMR User Should Know!
• Absolute Chemical Shift Referencing for "X"-Nucleus NMR Spectra (using the xref macro in VNMR) 
• Fluorine-19 Chemical Shift Reference Standards (table) 
• 2D NMR Processing in MestReNova - Quick-Start Guide